LogoConductLayer
Protective Topcoat2–4 µm · N/AElectroplated Nickel1–3 µm · 1.4×10⁷ S/mElectroless Copper0.3–0.8 µm · 5.8×10⁷ S/mActivation Seed Layer~10 nm · Pd catalystBase Substrate (PET)100–300 µm · Insulating
XSEC-001
12s LOOP
SCALE 1:50,000

Seven layers.
Fourteen chemistry
stages.
One fabric.

Copper bonded to polyester at the atomic level. Defense-grade EMI shielding, heated garment layers, and biocompatible conductive wound dressings — built to your exact specification.

Defense / EMI ShieldingWearable-Tech PrototypingMedical Device — ISO 10993MIL-STD-461 Certified
14
Chemistry Stages
per production run
7
Deposited Layers
base to topcoat
0.3 µm
Cu Deposit Tolerance
±0.05 µm
72 dB
SE @ 1 GHz
MIL-STD-461 verified
Scroll Process
STAGE 01·PT-01

Pre-Treatment

Surface preparation & organic removal

Every substrate enters a 3-bath alkaline cleaning sequence. Oils, sizing agents, and atmospheric contaminants are stripped to a contact angle below 20°. A substrate that isn't atomically clean at this stage will produce adhesion failures three layers later — this is where tolerances are either established or destroyed.

PT-01·Pre-Treatment
LIVE
Bath Temp
60°C
Range: 55–65°C
Soak Time
8min
Range: 6–12 min
pH
11.2
Range: 10.8–11.8
Detergent Conc.
12g/L
Range: 10–15 g/L
Bath 1
Alkaline Degreaser
TEMP
60°C
TIME
3 min
Removes oils & waxes
Bath 2
Anionic Surfactant
TEMP
55°C
TIME
3 min
Lifts fiber sizing
Bath 3
DI Water Rinse
TEMP
20°C
TIME
2 min
Zero-conductivity rinse
PT-01 Output vs. Industry Pre-Treatment StandardsConductLayer vs. Industry
MetricConductLayerIndustry Avg.Unit
Contact angle post-clean< 20°25–40°°
Residual organic contamination< 0.51.5–3.0mg/m²
Surface roughness (Ra)180–220300–500nm
Process repeatability (σ)< 2.15–8%
STAGE 02·AC-02

Activation

Palladium-tin catalyst seeding

Palladium-tin colloidal catalyst is adsorbed onto the cleaned fiber surface. The Pd²⁺ ions form the catalytic seed layer that will initiate electroless copper reduction in Stage 3. Seed density directly determines copper nucleation uniformity — at 1.8×10¹⁴ atoms/cm², we achieve a continuous film rather than isolated islands.

AC-02·Activation
LIVE
Pd Conc.
0.18g/L
Range: 0.15–0.22 g/L
Sn²⁺ Conc.
14g/L
Range: 12–18 g/L
Bath Temp
30°C
Range: 25–35°C
pH
1.8
Range: 1.5–2.2
AC-02 Seed Density vs. Industry Activation PerformanceConductLayer vs. Industry
MetricConductLayerIndustry Avg.Unit
Pd seed density1.8×10¹⁴0.9×10¹⁴atoms/cm²
Activation uniformity< 3.28–15% CV
Accelerator bath life420200–280cycles
STAGE 03·ED-03

Electroless Deposition

Autocatalytic copper reduction

In an alkaline formaldehyde-reducing bath, copper ions are reduced onto the palladium seed layer without external current. The reaction is autocatalytic — once started, the copper surface itself catalyzes further deposition. Controlling pH to ±0.2 units at 42°C is the single most critical variable in this stage; drift produces void formation and resistivity spikes.

ED-03·Electroless Deposition
LIVE
Cu²⁺ Conc.
3.2g/L
Range: 2.8–3.8 g/L
Formaldehyde
8mL/L
Range: 6–10 mL/L
Bath Temp
42°C
Range: 38–46°C
pH
12.4
Range: 12.0–12.8
Critical Parameter Alert
pH window: 12.0–12.8

Outside this window: below 12.0 → bath decomposition; above 12.8 → co-deposition of Cu₂O inclusions raising resistivity 18–40%.

Current pH
12.4
NOMINAL
ED-03 Deposit Quality vs. Electroless Industry BenchmarksConductLayer vs. Industry
MetricConductLayerIndustry Avg.Unit
Deposition rate2.41.2–1.8µm/hr
Copper purity99.496–98% Cu
Void density< 0.32–8voids/cm²
Thickness uniformity2.88–14% CV
STAGE 04·EP-04

Electroplating

Nickel overplate for durability & corrosion resistance

The electroless copper layer (0.3–0.8 µm) is overplated with electrodeposited nickel to 1–3 µm. Nickel provides corrosion barrier, hardness (520 HV vs. copper's 80 HV), and maintains shielding effectiveness through wash cycles. Current density at 2.4 A/dm² produces a fine-grained deposit; exceeding 3.5 A/dm² causes burning at fiber crossover points.

EP-04·Electroplating
LIVE
Current Density
2.4A/dm²
Range: 1.5–3.5 A/dm²
Ni²⁺ Conc.
82g/L
Range: 75–90 g/L
Bath Temp
52°C
Range: 48–58°C
Plating Time
18min
Range: 12–25 min
EP-04 Plated Performance vs. Competitor Final ProductsConductLayer vs. Industry
MetricConductLayerIndustry Avg.Unit
Surface resistance0.0420.12–0.25Ω/sq
Shielding effectiveness (1 GHz)7245–58dB
Nickel layer hardness520380–440HV
Tensile strength retention9782–90%
STAGE 05·QA-05

Quality Assurance

100% lot testing — no sampling protocols

Every production lot undergoes full four-point probe resistance mapping (25 measurement points per 1m² panel), ASTM D3359 adhesion tape test, and shielding effectiveness measurement per IEEE 299-2006. Medical-grade lots additionally undergo ISO 10993-5 cytotoxicity evaluation. We publish raw test data with every shipment.

QA-05·Quality Assurance
LIVE
Sheet Resistance
0.042Ω/sq
Range: < 0.05 Ω/sq
Adhesion (ASTM)
4B
Range: ≥ 3B
SE @ 1 GHz
72dB
Range: ≥ 65 dB
Thickness CV
2.1%
Range: < 5%
MIL-STD-461G
EMI/EMC Shielding
ISO 10993-5
Biocompatibility
IEEE 299-2006
SE Measurement
ASTM D3359
Adhesion Testing
RoHS 2.0
Material Compliance
REACH SVHC
Chemical Safety
QA-05 Compliance Rates vs. Industry Testing StandardsConductLayer vs. Industry
MetricConductLayerIndustry Avg.Unit
MIL-STD-461 pass rate99.287–92%
ISO 10993-5 cytotoxicityGrade 0Grade 1–2grade
Wash durability (cycles)> 10030–60cycles
Lot-to-lot resistance variance< 412–22%
STAGE 06·FN-06

Finishing

Protective topcoat application & cure

A 2–4 µm fluoropolymer or polyurethane topcoat is applied by pad-mangle and cured at 120°C. The topcoat maintains surface resistance below 0.05 Ω/sq while providing 500+ hour salt spray resistance (ASTM B117). Topcoat chemistry is selected based on end-use: PTFE-based for medical, PU for defense, silicone-hybrid for high-flex wearable applications.

FN-06·Finishing
LIVE
Topcoat Thickness
3.2µm
Range: 2–4 µm
Cure Temp
120°C
Range: 110–130°C
Cure Time
22min
Range: 18–28 min
Salt Spray (hrs)
500h
Range: ≥ 480 h
Medical Devices
PTFE-Based
Low flex
ISO 10993 compliant, zero cytotoxicity
Defense / EMI
Polyurethane
Medium flex
MIL-STD-810 environmental
Wearable Tech
Silicone Hybrid
High flex (>50k cycles)
Maintains SE after repeated bending
FN-06 Final Product Performance vs. Industry Finished GoodsConductLayer vs. Industry
MetricConductLayerIndustry Avg.Unit
Salt spray resistance500+200–350hours
Topcoat adhesion (ASTM D3359)5B3B–4Bgrade
Post-finish sheet resistance0.0480.15–0.30Ω/sq

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Download Full Process Spec Sheet

47 pages. Every bath formulation, operating window, control parameter, and test method. The same document we hand to defense procurement officers and FDA submission teams.

Complete bath chemistry formulations
Statistical process control charts (12-month data)
MIL-STD-461G test reports
ISO 10993-5 biocompatibility certificates
Lot traceability methodology
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